Mar 5, 2016 12:59
8 yrs ago
English term

then slowly taken to 22 °C

English to Russian Science Chemistry; Chem Sci/Eng
The mixture was stirred at 4 °C for 18h, then slowly taken to 22 °C. The mixture was again cooled to 0 °C and pentafluorophenol (2.01 g, 10.9 mmol) was added followed by a dropwise addition of Et3N (1.51 mL, 10.8 mmol).

Большое спасибо!!!
Votes to reclassify question as PRO/non-PRO:

Non-PRO (1): Igor Boyko

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Proposed translations

+7
3 mins
Selected

затем температуру (смеси) медленно довели до 22...

,

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Note added at 4 mins (2016-03-05 13:04:05 GMT)
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то есть, скорее всего, просто оставили стоять при комнатной температуре
Peer comment(s):

agree Edgar Hermann
12 mins
спасибо!
agree cherepanov
2 hrs
спасибо
agree Vladimir Bragilevsky
2 hrs
спасибо
agree Natalie
3 hrs
спасибо!
agree Vladimir Vaguine
3 hrs
спасибо!
agree Tatiana Lammers
6 hrs
спасибо!
agree Leon Ivanihin
20 hrs
спасибо!
Something went wrong...
4 KudoZ points awarded for this answer.
+1
3 mins

затем медленно нагревается до 22 °c

...
Peer comment(s):

agree Margarita Vidkovskaia
7 hrs
Something went wrong...
+2
3 mins

медленно довели температуру смеси до 22°C

.
Peer comment(s):

agree Edgar Hermann
12 mins
Thank you, Edgar!
agree Larisa Horback
11 hrs
Something went wrong...
6 mins

затем температуру (смеси) медленно подняли до 22 °C

...
Something went wrong...
+1
7 hrs

после чего была медленно нагрета до 22°C

Смесь перемешивалась в течение 18 часов при 4°C , после чего была медленно нагрета до 22°C.
Peer comment(s):

agree Larisa Horback
3 hrs
Спасибо
Something went wrong...
11 hrs

постепенно нагрели до 22 °c

можно "со временем довели температуру смеси до 22°c"
Something went wrong...
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